Refining

DEGUMMING

Water Degumming

A large part of the gums can be hydrated quickly and easily. Crude oil is pumped continuously to an in line mixer where in pre-calculated quantity of water is added. Oil water mixture is fed to the hydration tank and allowed sufficient resident time for the gums to agglomerate on hydration and pumped to Separator where the oil and hydrated gums are separated and pumped to storage. Some particles that are not removed by water degumming need Acid Treatment.

Acid Degumming

In some oils, the gums are not hydrated properly, in such cases, acid degumming is used. Phosphoric acid is mixed with the oil and allowed sufficient resident time. These acid hydrated gums are then removed by centrifugal separators.

Salient features

  • Water degumming can be carried out in the Extraction Plant.
  • The separated gums are added to the deoiled meal in the toaster.
  • To produce lecithin, these gums are dried separately.

NEUTRALIZING

Neutralization is a chemical process for separating the free fatty acids from oils using Caustic.
The neutralized oil is to be washed before bleaching to separate any traces of soap or acid from oil.
After washing, the oil is vacuum dried to remove any water traces.

Degummed oil after conditioning is fed into the mixer where it is mixed with calculated quantity of caustic soda solution of suitable strength. Free fatty acids in the oil react with caustic soda to form soap. The mixture of oil and soap along with the precipitated gums is fed into a Centrifuge/Seperator to separate oil and soap stock.

Washing & Vacuum Drying

Neutralized oil produced from the separator still contains soap and needs to be washed. Hot water is added to the neutral oil and mixed in the mixer. The washed water and neutral oil are separated in the Seperator. The washed oil from separator is dried continuously in the vacuum drier.

Salient features

  • Easily transforms free fatty acids into soap
  • Removal of phospholipids that are not hydrated at degumming level
  • Removal of metals, pigments and other volatiles.

DEWAXING/WINTERISING

  • Sunflower, Corn and Rice bran oil is to be Dewaxed/Winterised before consumption as it contains high molecular weight wax. If oils stored at low temperatures , waxes, high melting tri glycerides and certain gums may separate as solids from the oil. This leads to an undesirable cloudy appearance , and many consumers may mistakenly think the oil is spoiled.
  • To obtain very clear quality of oil specially in cold conditions, oil needs to be dewaxed/winterized.
  • The oil is cooled in crystallisers and gradually the crystal formation takes place. Here filter aid is also added.
  • The oil is then transferred to a maturator where the crystals are allowed to grow. The oil is continuously cooled by the help of glycol water flowing through the coils.
  • Finally the oil is filtered on hermetic pressure leaf filters to remove the waxes.
  • For Rice bran oil, Veendeep has developed PP Filters which are more suitable for high wax oil.

Salient features

  • Single plant can be used for Dewaxing and Winterising.
  • Optimum care is taken to maintain the formed crystals till filtration.
  • Minimum filter aid consumption.

REFINING

Majority of the crude oil obtained from pressing or solvent extraction contains impurities and these are to be removed to make the oil suitable for human consumption. Depending on the type of oil, the preparation of seeds and extraction process used, vegetable oil contains various impurities. These impurities have a negative effect on the taste, odour and appearance of the oil and hence have to be removed. Veendeep’s most modern refinery is used for capacities ranging from 30 TPD to 500 TPD . Oils have different levels of Free Fatty Acids(FFA) and hence need to be treated differently. Based on this there are two types of refining process:

TYPES OF REFINING PROCESS

BLEACHING

The main purpose of bleaching is to remove coloring matters by absorption to obtain finished product with the desired color, on the other hand, for conventional refining, bleaching serves also to eliminate traces of soap before oil is passed to the final stage of deodorization.

The degummed/neutralized oil is first heated to desired temperature and then bleaching earth is added in adequate quantity controlled by PLC into the Oil – Earth mixer under vacuum.

This mixture of oil and earth is then pumped to Bleacher where it is agitated by open sparge steam and uniform bleaching takes place.

This is then transferred to Pressure leaf filters where the spent earth ( Cake) is separated and filtered again by passing oil through polish filters.

Salient features

  • Uniform holding time of the oil-earth mixture in the bleacher.
  • Oil filtration in hermetic leaf filters that requires
    no maintenance.
  • Savings of both labor and floor space, as well
    as in a lower bleaching
    earth consumption to obtain the same bleaching result.
  • Accurate and convenient metering of oil and earth for obtaining quickly
    oil of the desired color.
  • Filtered oil is kept under vacuum during whole process.
  • The bleacher is totally maintenance free as there are no mechanical agitators.
  • Oil content in spent earth (cake) not exceeding 24%.

DEODORIZING

Deodorising is the final stage of the refining process and it is used to free the bleached/dewaxed oil from odoriferous material, free fatty acids and other minor impurities present.
Veendeep Oiltek’s special Deordorisation plant processes bleached oil to give superior quality odorless, colorless, bland oil with good shelf life.

The bleached oil is first pumped into Deareator where entrapped air if any is removed. The oil is then heated in vacuum final heater to the required deodorizing temperatures with the help of high pressure steam/ Thermic Fluid heating system.

The oil flows into the trays of the Deodorizer along longitudinal channels. Sparge steam pipes are installed in each compartment for intimate mixing of the oil and the steam.
The oil then flows to subsequent many deodorizing trays and then finally enters into the heat recovery tray.The oil is then cooled in the heat exchanger .

The deodorized oil then passes through a set of polish filters for storage.
The fatty acids and other components pass through large ducts and are condensed in special condensing section by means of fatty acids circulating at low temperature.

Salient features

  • Heating and cooling the oil is done under vacuum ensuring high quality and no side products.
  • Efficient heat recovery of more than 80% ensuring low energy consumption.
  • Shallow bed design for intricate mixing of steam and oil.
  • Efficient scrubbing of the fatty acids for low carry over to the hot wells.